1. chem960
  2. 82373-94-2
2,3,5,4'-Tetrahydroxy stilbene-2-Ο-β-D-glucoside | 82373-94-2

Nom du produit:2,3,5,4'-Tetrahydroxy stilbene-2-Ο-β-D-glucoside

Numéro CAS:82373-94-2
Le MF:C20H22O9
Mégawatts:406.383286952972
MDL:MFCD00238694
Zone centrale d'information:60430
PubChem id:5321884
Présentation
   Le stilbénoside est l'un des principaux ingrédients de Ho huau Koko ho huau. C'est un composé polyhydroxyphénolique. A un effet antioxydant, élimine les radicaux libres. C'est également un ingrédient efficace pour lutter contre le vieillissement et réduire les lipides sanguins, avec une grande valeur de recherche
Nom et identifiant
  • 2,3,5,4'-Tetrahydroxy stilbene-2-Ο-β-D-glucoside
  • 2,3,5,4'-Tetrahydroxystilbene-2-O-beta-D-glucopyranoside
  • 2,3,5,4'-tetera-hydroxystilbene-2-O-β-D-glucoside
  • 2,3,4',5-Tetrahydroxystilbene 2-O-D-glucoside
  • 2,3,5,4' -tetrahydroxystibene -2-O-β-D –glucoside
  • 2,3,5,4-tetrahydroxyldiphenylethylene-2-o-glucoside
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-glucoside
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-glucoside
  • 2,3,5,4'-TETRAHYDROXYSTILBENE-2-O-B-D-GLUCOPYRANOSIDE
  • b-D-Glucopyranoside,2,4-dihydroxy-6-[(1E)-2-(4-hydroxyphenyl)ethenyl]phenyl
  • CIS,2,3,5,4-tetrahydroxyl diphenylethylene-2-o-glucoside
  • 2,3,4,5,6-PENTAFLUOROPHENYL4-BROMO-2-CHLOROBENZENESULFONATE
  • 2,3,5,4'-tetera-hydroxystilbenen-2-O-Beta-D-glucoside
  • 2,3,5,4'-tetrahydroxystibene-2-O-Beta-D glucoside
  • 2,3,5,4'-Tetrahydroxystilbene-2-O-β-D-glucopyranoside
  • 2,4-Dihydroxy-6-[(1E)-2-(4-hydroxyphenyl)ethenyl]phenyl β-D-Glucopyranoside
  • EH-201
  • THSG
  • Tetrahydroxystilbene glucoside
  • 2,3,5,4′-Tetrahydroxystilbene 2-O-β-D-glucoside
  • 2,3,5,4'-Tetrahydroxy;stilbene-2-Ο-β-D- glucoside
  • Tetrahydroxystilbene Glucoside
  • 2,3,5,4'-Tetra-hydroxystilbene-2-O-beta-D-glucopyranoside
  • Astragalus polyphenols
  • 2,3,5,4-tetrahydroxyl diphenylethylene-2-o-glucoside
  • 54QRI6OKJ5
  • 2,3,5,4'-Tetrahydroxystilbene-2-O-beta-D-glucoside
  • (2S,3R,4S,5S,6R)-2-(2,4-dihydroxy-6-((E)-4-hydroxystyryl)phenoxy)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol
  • (2S,3R,4S,5S,6R)-2-[2,4-dihydroxy-6-[(E)-2-(4-hydroxyphenyl)ethenyl]phenoxy]-6-(hydroxymeth
  • (2S,3R,4S,5S,6R)-2-[2,4-dihydroxy-6-[(E)-2-(4-hydroxyphenyl)ethenyl]phenoxy]-6-(hydroxymethyl)oxane-
  • 2,4-Dihydroxy-6-[(1E)-2-(4-hydroxyphenyl)ethenyl]phenyl β-D-glucopyranoside (ACI)
  • β-D-Glucopyranoside, 2,4-dihydroxy-6-[2-(4-hydroxyphenyl)ethenyl]phenyl, (E)- (ZCI)
  • (E)-2,3,5,4′-Tetrahydroxy stilbene-2-O-glucoside
  • 2,3,4′,5-Tetrahydroxystilbene 2-O-D-glucoside
  • trans-2,3,5,4′-Tetrahydroxystilbene-2-O-β-d-glucopyranoside
  • 2,3,5,4'-Tetrahydroxystilbene 2-O--D-glucoside
  • MFCD00238694
  • CCG-268716
  • AfAE'Adaggeratrade markAfA centA centasA notA em leaderA inverted exclamation mark-D-glucoside
  • SCHEMBL2688101
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-glucosid
  • 2,3,5,4'-Tetrahydroxytoluylene-2-beta-D-glucopyranoside
  • 2,4-dihydroxy-6-[(E)-2-(4-hydroxyphenyl)ethenyl]phenyl beta-D-glucopyranoside
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-fA-D-Glucoside
  • Q-100633
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-b-D-glucoside
  • 2,3,5,4'-Tetrahydroxytoluylene-2-beta-D-glucoside
  • CHEBI:140850
  • tetrahydroxyldiphenylethylene-2-o-glucoside
  • s3906
  • (E)-2,3,5,4'-tetrahydroxystilbene-2-O-beta-D-glucoside
  • 2,3,5,4'-Tetrahydroxyl diphenylethylene-2-O-glucoside
  • 2,3,5,4'-TETRAHYDROXYSTILBENE-2-O-.BETA.-D-GLUCOSIDE
  • AC-33974
  • F16062
  • 2,3,5,4'-Tetrahydroxy stilbene-2---D-glucoside
  • 2,3,5,4'-tetrahydroxystilbene 2-O-beta-D-glucoside
  • trans-2,3,5,4'-tetrahydroxystilbene-2-O-beta-D-glucoside
  • DTXSID801242061
  • AKOS030530177
  • (2S,3R,4S,5S,6R)-2-[2,4-dihydroxy-6-[(E)-2-(4-hydroxyphenyl)ethenyl]phenoxy]-6-(hydroxymethyl)oxane-3,4,5-triol
  • 2,3,5,4-tetrahydroxyl-diphenylethylene-2-o-glucoside
  • UNII-54QRI6OKJ5
  • 2,3,5,4'-tetrahydroxystilbene-2-o-beta-d-glucopyranoside
  • 55327-45-2
  • NCGC00482790-01
  • A864422
  • BDBM50020713
  • 2,3,5,4'-TETRAHYDROXYSTILBENE-2-O-BETA-D-GLUCOSIDE (USP-RS)
  • T3513
  • W-203871
  • 2,3,5,4'-TETRAHYDROXYSTILBENE-2-O-BETA-D-GLUCOSIDE [USP-RS]
  • SCHEMBL17507729
  • 2,4-DIHYDROXY-6-((1E)-2-(4-HYDROXYPHENYL)ETHENYL)PHENYL .BETA.-D-GLUCOPYRANOSIDE
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-AfAE'A centa' notA inverted exclamation markAfasA'A
  • 2,3,5,4-Tetrahydroxy stilbene-2-Omicron-beta-D-glucoside
  • beta-D-Glucopyranoside, 2,4-dihydroxy-6-((1E)-2-(4-hydroxyphenyl)ethenyl)phenyl
  • 2,3,5,4'-Tetrahydroxyl-diphenylethylene-2-O-beta-D-glucoside
  • tetrahydroxyl diphenylethylene-2-o-gluco
  • 2,3,4',5-Tetrahydroxystilbene 2-o-D-glucoside
  • CHEMBL460860
  • 2,3,5,4'-Tetrahydroxystilbene-2-O-ss-D-glucoside
  • AKOS040758637
  • 82373-94-2
  • B-D-GLUCOPYRANOSIDE,2,4-DIHYDROXY-6-[2-(4-HYDROXYPHENYL)ETHENYL]PHENYL
  • tetrahydroxystilbene glucoside
  • 2,3,5,4'-Tetrahydroxystilbene-2-O-b-D-glucopyranoside
  • 2,4-Dihydroxy-6-((1E)-2-(4-hydroxyphenyl)ethenyl)phenyl beta-D-glucopyranoside
  • beta-D-Glucopyranoside, 2,4-dihydroxy-6-(2-(4-hydroxyphenyl)ethenyl)phenyl
  • Tetrahydroxystilbene-2-O-??-D-glucoside
  • (2S,3R,4S,5S,6R)-2-[2,4-dihydroxy-6-[(E)-2-(4-hydroxyphenyl)vinyl]phenoxy]-6-(hydroxymethyl)tetrahydropyran-3,4,5-triol
  • 2,3,4',5-Tetrahydroxystilbene 2-O-Glucoside
  • .BETA.-D-GLUCOPYRANOSIDE, 2,4-DIHYDROXY-6-((1E)-2-(4-HYDROXYPHENYL)ETHENYL)PHENYL
  • .BETA.-D-GLUCOPYRANOSIDE, 2,4-DIHYDROXY-6-(2-(4-HYDROXYPHENYL)ETHENYL)PHENYL, (E)-
  • beta-D-Glucopyranoside, 2,4-dihydroxy-6-(2-(4-hydroxyphenyl)ethenyl)phenyl, (E)-
  • (E)-2,3,5,4'-Tetrahydroxy stilbene-2-O-glucoside
  • 2,3,5,4'-tetrahydroxystilbene-2-O-?-D-glucoside
  • AS-76404
  • [ "" ]
  • 2,3,4',5-Tetrahydroxystilbene 2-O-beta-D-glucopyranoside
  • 2,3,5,4'-tetrahydroxystilbene-2-O-beta-D-glucoside
  • MDL:MFCD00238694
  • InChIKey:JAYVHSBYKLLDJC-DSNJPTTOSA-N
  • Inchi:1S/C20H22O9/c21-9-15-16(25)17(26)18(27)20(28-15)29-19-11(7-13(23)8-14(19)24)4-1-10-2-5-12(22)6-3-10/h1-8,15-18,20-27H,9H2/b4-1+/t15-,16-,17+,18-,20+/m1/s1
  • SMILES:O([C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1)C1=C(O)C=C(O)C=C1/C=C/C1C=CC(O)=CC=1
Propriétés chimiques et physiques

Propriétés calculées

  • Qualité précise: 406.4g/mol
  • Charge de surface: 0
  • XLogP3: 1
  • Nombre de donneurs de liaisons hydrogène: 7
  • Nombre de récepteurs de liaison hydrogène: 9
  • Nombre de liaisons rotatives: 5
  • Masse isotopique unique: 406.126382g/mol
  • Masse isotopique unique: 406.126382g/mol
  • Surface topologique des pôles: 160Ų
  • Comptage des atomes lourds: 29
  • Complexité: 536
  • Comptage atomique isotopique: 0
  • Nombre de stéréocentres atomiques définis: 5
  • Nombre non défini de stéréocentres atomiques: 0
  • Nombre de centres stéréoscopiques d'obligations fixes: 1
  • Nombre indéfini de centres stéréoscopiques bond: 0
  • Nombre d'unités de liaison covalente: 1

Propriétés expérimentales

  • Le LogP: 0.15250
  • Le PSA: 160.07000
  • Solubilité: H2O: soluble5mg/mL, clear (warmed)
  • Couleur / forme: Powder
  • Point d'ébullition: 715°C at 760 mmHg
  • Indice de réfraction: 1.76
  • Point d'éclair: 386.2°C
  • Dense: 1.593g/cm3
Informations de sécurité
  • Symbolisme: GHS07
  • Wgk Allemagne:3
  • Instructions de sécurité:26
  • Signe de marchandises dangereuses: Xi Xi
  • Numéro de transport des marchandises dangereuses:NONH for all modes of transport
  • Description des dangers:H315-H319
  • Déclaration d'avertissement:P305+P351+P338
  • Conditions de stockage:Powder -20°C 3 years   4°C 2 years In solvent -80°C 6 months   -20°C 1 month
  • Code de catégorie de danger:36/38
  • Mot signal:Warning
Circuits synthétiques

Circuits synthétiques 1

Conditions de réaction
1.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
1.2 rt; 12 h, rt
1.3 Solvents: Water ;  rt
2.1 Reagents: Sodium borohydride Solvents: Methanol ;  30 min, rt
2.2 Reagents: Hydrochloric acid Solvents: Water ;  rt
3.1 Reagents: Carbon tetrabromide ,  Triphenylphosphine Solvents: Diethyl ether ;  rt
4.1 Solvents: Toluene ;  12 h, reflux
5.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
5.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
5.3 Solvents: Water ;  rt
6.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
6.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
7.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
7.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 2

Conditions de réaction
1.1 Reagents: Carbon tetrabromide ,  Triphenylphosphine Solvents: Diethyl ether ;  rt
2.1 Solvents: Toluene ;  12 h, reflux
3.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
3.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
3.3 Solvents: Water ;  rt
4.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
4.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
5.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
5.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 3

Conditions de réaction
1.1 Reagents: Sodium borohydride Solvents: Methanol ;  30 min, rt
1.2 Reagents: Hydrochloric acid Solvents: Water ;  rt
2.1 Reagents: Carbon tetrabromide ,  Triphenylphosphine Solvents: Diethyl ether ;  rt
3.1 Solvents: Toluene ;  12 h, reflux
4.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
4.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
4.3 Solvents: Water ;  rt
5.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
5.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
6.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
6.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 4

Conditions de réaction
1.1 Reagents: Potassium carbonate Solvents: Acetone ;  reflux
2.1 Reagents: Hydrogen peroxide Catalysts: Sulfuric acid Solvents: Methanol ,  Water ;  2 h, rt
2.2 Solvents: Water ;  rt
3.1 Solvents: Acetic acid ,  Dimethylformamide ;  3 h, reflux
3.2 Solvents: Water
4.1 Reagents: Sodium hydroxide Catalysts: Tetrabutylammonium bromide Solvents: Dichloromethane ,  Water ;  12 h, 65 - 70 °C
4.2 Solvents: Water
5.1 Reagents: Hydrogen Catalysts: Palladium Solvents: Ethyl acetate ;  16 h, 45 psi, rt
6.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
7.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
7.2 rt; 15 h, rt
7.3 Solvents: Water ;  rt
8.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
8.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
8.3 Solvents: Water ;  rt
9.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
9.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
10.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
10.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 5

Conditions de réaction
1.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
1.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
2.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
2.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 6

Conditions de réaction
1.1 Reagents: Hydrogen Catalysts: Palladium Solvents: Ethyl acetate ;  16 h, 45 psi, rt
2.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
3.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
3.2 rt; 15 h, rt
3.3 Solvents: Water ;  rt
4.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
4.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
4.3 Solvents: Water ;  rt
5.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
5.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
6.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
6.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 7

Conditions de réaction
1.1 Solvents: Acetic acid ,  Dimethylformamide ;  3 h, reflux
1.2 Solvents: Water
2.1 Reagents: Sodium hydroxide Catalysts: Tetrabutylammonium bromide Solvents: Dichloromethane ,  Water ;  12 h, 65 - 70 °C
2.2 Solvents: Water
3.1 Reagents: Hydrogen Catalysts: Palladium Solvents: Ethyl acetate ;  16 h, 45 psi, rt
4.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
5.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
5.2 rt; 15 h, rt
5.3 Solvents: Water ;  rt
6.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
6.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
6.3 Solvents: Water ;  rt
7.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
7.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
8.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
8.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 8

Conditions de réaction
1.1 Solvents: Toluene ;  12 h, reflux
2.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
2.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
2.3 Solvents: Water ;  rt
3.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
3.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
4.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
4.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 9

Conditions de réaction
1.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
2.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
2.2 rt; 15 h, rt
2.3 Solvents: Water ;  rt
3.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
3.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
3.3 Solvents: Water ;  rt
4.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
4.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
5.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
5.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 10

Conditions de réaction
1.1 Reagents: Sodium hydroxide Catalysts: Tetrabutylammonium bromide Solvents: Dichloromethane ,  Water ;  12 h, 65 - 70 °C
1.2 Solvents: Water
2.1 Reagents: Hydrogen Catalysts: Palladium Solvents: Ethyl acetate ;  16 h, 45 psi, rt
3.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
4.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
4.2 rt; 15 h, rt
4.3 Solvents: Water ;  rt
5.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
5.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
5.3 Solvents: Water ;  rt
6.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
6.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
7.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
7.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 11

Conditions de réaction
1.1 Catalysts: Water Solvents: Methanol ;  0.5 h
Référence
Water-Assisted/Water-Accelerated Photoreaction of trans-2,3,4',5-Tetrahydroxystilbene-2-O-β-D-glucoside from the Roots of Polygonum multiflorum
Bao, Ni-Man ; et al, Journal of Agricultural and Food Chemistry, 2020, 68(18), 5086-5092

Circuits synthétiques 12

Conditions de réaction
1.1 Reagents: Hydrogen peroxide Catalysts: Sulfuric acid Solvents: Methanol ,  Water ;  2 h, rt
1.2 Solvents: Water ;  rt
2.1 Solvents: Acetic acid ,  Dimethylformamide ;  3 h, reflux
2.2 Solvents: Water
3.1 Reagents: Sodium hydroxide Catalysts: Tetrabutylammonium bromide Solvents: Dichloromethane ,  Water ;  12 h, 65 - 70 °C
3.2 Solvents: Water
4.1 Reagents: Hydrogen Catalysts: Palladium Solvents: Ethyl acetate ;  16 h, 45 psi, rt
5.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
6.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
6.2 rt; 15 h, rt
6.3 Solvents: Water ;  rt
7.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
7.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
7.3 Solvents: Water ;  rt
8.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
8.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
9.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
9.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 13

Conditions de réaction
1.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
1.2 rt; 15 h, rt
1.3 Solvents: Water ;  rt
2.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
2.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
2.3 Solvents: Water ;  rt
3.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
3.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
4.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
4.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 14

Conditions de réaction
1.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
1.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
1.3 Solvents: Water ;  rt
2.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
2.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
3.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
3.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Circuits synthétiques 15

Conditions de réaction
1.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
1.2 Solvents: Water ;  rt
Référence
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301
Littérature connexe
  • 1. Enhanced TSG stability through co-assembly with C3G: the mechanism behind processing Polygonum multiflorum Thunb with black beans via supramolecular analysis Yue Liu,Shukai Wang,Yunan Qin,Ying Wang,Jianbo Yang,Lanzhen Zhang,Quan Li,Shuangcheng Ma Food Funct. 2023 14 4204
Produits connexes
Données de prix disponibles
La marque:Mce Fournisseurs:MedChemExpress
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
HY-N0652-10mM*1mLinDMSO 99.20% In-stock 10mM*1mLinDMSO ¥550 26 Jul. 2023
HY-N0652-10mg 99.20% In-stock 10mg ¥500 01 Sep. 2023
HY-N0652-25mg 99.20% In-stock 25mg ¥1000 01 Sep. 2023
HY-N0652-50mg 99.20% In-stock 50mg ¥1400 01 Sep. 2023
HY-N0652-5mg 99.20% In-stock 5mg ¥312 01 Sep. 2023
HY-N0652-10mM*1 mL in DMSO 99.20% In-stock 10mM*1 mL in DMSO ¥550 01 Sep. 2023
La marque:sigmaaldrich Fournisseurs:西格玛奥德里奇(上海)贸易有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
1651654-50MG 50mg ¥5141.51 06 Sep. 2023
PHL82666-10MG 10mg ¥4932.81 09 Sep. 2023
1651654-50MG 50MG ¥4896.69 12 Apr. 2023
PHL82666-10MG 10MG ¥4697.92 06 Jan. 2023
La marque:topscience Fournisseurs:上海陶术生物科技有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
T2964-10 mg 99.77% 上海现货 10mg ¥410.00 26 Apr. 2022
T2964-1 mL * 10 mM (in DMSO) 99.77% 上海现货 1 mL * 10 mM (in DMSO) ¥410.00 26 Apr. 2022
T2964-100 mg 99.77% 上海现货 100MG ¥1730.00 26 Apr. 2022
T2964-50 mg 99.77% 上海现货 50mg ¥1156.00 26 Apr. 2022
T2964-25 mg 99.77% 上海现货 25mg ¥811.00 26 Apr. 2022
La marque:scbt Fournisseurs:圣克鲁斯生物技术
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
sc-283376-500mg 500mg ¥6017.00 05 Sep. 2023
sc-283376A-2g 2g ¥12974.00 05 Sep. 2023
sc-283376A-2 g 2g ¥12,974.00 10 Jul. 2023
sc-283376-500 mg 500MG ¥6,017.00 10 Jul. 2023
La marque:chemfaces Fournisseurs:ChemFaces
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
CFN99995-20mg >=98% 20mg $30/ ¥217.90 19 Sep. 2023
CFN99995-20mg >=98% 20mg $40/ ¥290.53 22 Jul. 2021
La marque:安捷凯 Fournisseurs:武汉安捷凯生物医药科技有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
ajcn5494-20mg 98% 现货 20mg ¥1269.00 07 Sep. 2023
La marque:Acmec Fournisseurs:上海吉至生化科技有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
T88670-1g 现货 1g ¥3498.0 07 Sep. 2021
T88670-20mg 现货 20mg ¥278.0 07 Sep. 2021
La marque:源叶 Fournisseurs:上海源叶生物科技有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
B21757-1g 分析标准品,HPLC≥98% 上海:准现货/北京:0/武汉:0/南京:0 1g ¥3500.00 02 Sep. 2021
B21757-20mg 分析标准品,HPLC≥98% 上海:>10/北京:2/武汉:4/南京:3 20mg ¥280.00 02 Sep. 2021
La marque:罗恩试剂 Fournisseurs:上海易恩化学技术有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
R027737-20mg 98%(分析标准试剂) 现货 20mg ¥338 07 Sep. 2023
R097435-500mg 99% 现货 500mg ¥654 07 Sep. 2023
R097435-100mg 99% 现货 100mg ¥204 07 Sep. 2023
La marque:dcchemical Fournisseurs:DC Chemicals
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
DCS-029-20 mg >98%, Standard References Grade In stock 20mg $280.0/ ¥2,033.70 01 Mar. 2022
DCS-029-20mg >98%, Standard References Grade In stock 20mg $280.0/ ¥2,033.70 15 Sep. 2023
La marque:bomeibio Fournisseurs:合肥博美生物科技有限责任公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
BZP0269-20mg HPLC≥98% 现货 20mg ¥320元 15 Sep. 2023
La marque:aladdin Fournisseurs:上海阿拉丁生化科技股份有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
T110192-20mg 分析标准品,>98% 现货 20mg ¥352.90 01 Sep. 2023
La marque:九鼎 Fournisseurs:上海贤鼎生物科技有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
CG191-5mg 95+% 3~5天 5mg 542CNY 08 May. 2021
CG191-10mg 95+% 3~5天 10mg 898CNY 08 May. 2021
CG191-25mg 95+% 3~5天 25mg 1797CNY 08 May. 2021
La marque:a2bchem Fournisseurs:A2B Chem LLC
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
AC37593-250mg ≥98% in stock 250mg $510.00/ ¥3,704.23 30 Dec. 2023
AC37593-50mg 99% in stock 50mg $112.00/ ¥813.48 30 Dec. 2023
AC37593-25mg 99% in stock 25mg $80.00/ ¥581.06 30 Dec. 2023
AC37593-10mg 99% in stock 10mg $40.00/ ¥290.53 30 Dec. 2023
AC37593-5mg 99% in stock 5mg $26.00/ ¥188.84 30 Dec. 2023
La marque:aaron Fournisseurs:Aaron
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
AR00546D-5g 98% In China Stock 5g $517.00/ ¥3,755.07 13 Dec. 2023
AR00546D-1g 98% In China Stock 1g $130.00/ ¥944.22 13 Dec. 2023
AR00546D-250mg 98% In China Stock 250mg $57.00/ ¥414.00 13 Dec. 2023
AR00546D-100mg 98% In China Stock 100mg $31.00/ ¥225.16 13 Dec. 2023
La marque:phytolab Fournisseurs:PhytoLab
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
82666-1000mg ≥ 95.0 % 1000mg €13800/ ¥100,066.56 25 Oct. 2023
82666-500mg ≥ 95.0 % 500mg €7360/ ¥53,368.83 25 Oct. 2023
82666-250mg ≥ 95.0 % 250mg €3910/ ¥28,352.19 25 Oct. 2023
82666-50mg ≥ 95.0 % 50mg €827.9999999999999/ ¥6,003.99 25 Oct. 2023
La marque:nstchemcial Fournisseurs:Nature Science Technologies
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
NST-10-1-25g 98% (HPLC) 25g € 520/ ¥3,770.62 21 Sep. 2023
NST-10-1-10g 98% (HPLC) 10g € 230/ ¥1,667.78 21 Sep. 2023
NST-10-1-5g 98% (HPLC) 5g € 160/ ¥1,160.19 21 Sep. 2023
NST-10-1-2.52,5g 98% (HPLC) 2.52,5g € 110/ ¥797.63 21 Sep. 2023
NST-10-1-25 g 98% (HPLC) 25g € 520/ ¥3,770.62 10 Jul. 2023
NST-10-1-10 g 98% (HPLC) 10g € 230/ ¥1,667.78 10 Jul. 2023
NST-10-1-5 g 98% (HPLC) 5g € 160/ ¥1,160.19 10 Jul. 2023
NST-10-1-2,5 g 98% (HPLC) 2,5 g € 110/ ¥797.63 10 Jul. 2023
La marque:abcr Fournisseurs:abcr
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
AB294879-1g 1g €242.80/ ¥1,760.59 08 Sep. 2023
AB294879-250mg 250mg €141.50/ ¥1,026.04 08 Sep. 2023
AB294879-1 g 1 g €242.80/ ¥1,760.59 20 Jul. 2023
AB294879-250 mg 250 mg €141.50/ ¥1,026.04 20 Jul. 2023
La marque:targetmol Fournisseurs:TargetMol Chemicals
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
T2964-1 mL * 10 mM (in DMSO) 99.77% 上海现货 1 mL * 10 mM (in DMSO) ¥ 410 11 Jul. 2023
T2964-100 mg 99.77% 上海现货 100MG ¥ 1,730 11 Jul. 2023
T2964-50 mg 99.77% 上海现货 50mg ¥ 1,156 11 Jul. 2023
T2964-25 mg 99.77% 上海现货 25mg ¥ 811 11 Jul. 2023
T2964-10 mg 99.77% 上海现货 10mg ¥ 410 11 Jul. 2023
La marque:enovation Fournisseurs:eNovation Chemicals LLC
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
Y1291321-1g 98% 1g $215/ ¥1,561.59 17 May. 2023
D659438-20mg 98% 20mg $285/ ¥2,070.01 03 Sep. 2023
La marque:TCI Fournisseurs:梯希爱(上海)化成工业发展有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
T3513-250MG >98.0%(HPLC) 上海:请联系我们/天津:请联系我们/日本:20 250mg ¥1100.00 07 Sep. 2023
T3513-50MG >98.0%(HPLC) 上海:请联系我们/天津:请联系我们/日本:10 50mg ¥350.00 07 Sep. 2023
La marque:麦克林 Fournisseurs:上海麦克林生化科技有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
T874838-1g 99% 预计交期:8~10个工作日 1g ¥1,692.00 28 Sep. 2022
T874838-500mg 99% 预计交期:1个工作日 500mg ¥1,128.00 28 Sep. 2022
T874838-100mg 99% 上海仓库:现货/北方仓库:现货/南方仓库:- 100mg ¥310.00 28 Sep. 2022
La marque:韶远 Fournisseurs:上海韶远试剂有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
SY022367-10mg 98% 10mg ¥405.0 15 Sep. 2023
La marque:百灵威 Fournisseurs:百灵威科技有限公司
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
910360-22MG 22MG ¥ 377 26 Apr. 2022
928007-5MG 98% 河北: 4 5MG ¥ 125 26 Apr. 2022
La marque:Biopurify Fournisseurs:Chengdu Biopurify Phytochemicals Ltd
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
BP0039-20mg 98% 20mg $40/ ¥290.53 20 Sep. 2023
BP0039-100mg 98% 100mg $80/ ¥581.06 20 Sep. 2023
BP0039-1000mg 98% 1000mg $160/ ¥1,162.11 20 Sep. 2023
La marque:1pchem Fournisseurs:1PlusChem
Non. Pureté Stocks Spécifications Prix Temps de mise à jour Fonctionnement
1P0053Y1-250mg ≥98% 1 week 250mg $651.00/ ¥4,728.34 16 Dec. 2023
1P0053Y1-100mg ≥98% 1 week 100mg $335.00/ ¥2,433.17 16 Dec. 2023
1P0053Y1-50mg 99% 1 week 50mg $191.00/ ¥1,387.27 16 Dec. 2023
1P0053Y1-25mg ≥98% 1 week 25mg $138.00/ ¥1,002.32 16 Dec. 2023
1P0053Y1-10mg 99% 1 week 10mg $91.00/ ¥660.95 16 Dec. 2023
1P0053Y1-5mg 99% 1 week 5mg $81.00/ ¥588.32 16 Dec. 2023
Les données ci - dessus proviennent toutes d'Internet. En cas d'atteinte à la vie privée, contactez - nous dès que possible (laissez une copie de l'e - mail de votre entreprise) et nous l'enregistrerons pour le traitement! Désolé pour le désagrément!
©2008-2024 chem960.com Tous droits réservés