1. chem960
  2. 82373-94-2
2,3,5,4'-Tetrahydroxy stilbene-2-Ο-β-D-glucoside | 82373-94-2

Product name:2,3,5,4'-Tetrahydroxy stilbene-2-Ο-β-D-glucoside

CAS No:82373-94-2
MF:C20H22O9
MW:406.383286952972
MDL:MFCD00238694
CID:60430
PubChem ID:5321884
Introduction
   Stilbene glycoside is one of the main components of Polygonum multiflorum, Polygonaceae. It is a kind of polyhydroxy phenolic compounds. It has the function of anti-oxidation and scavenging free radicals. It is also an effective component of anti-aging and Hypolipidemia, and has great research value
Names and Identifiers
  • 2,3,5,4'-Tetrahydroxy stilbene-2-Ο-β-D-glucoside
  • 2,3,5,4'-Tetrahydroxystilbene-2-O-beta-D-glucopyranoside
  • 2,3,5,4'-tetera-hydroxystilbene-2-O-β-D-glucoside
  • 2,3,4',5-Tetrahydroxystilbene 2-O-D-glucoside
  • 2,3,5,4' -tetrahydroxystibene -2-O-β-D –glucoside
  • 2,3,5,4-tetrahydroxyldiphenylethylene-2-o-glucoside
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-glucoside
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-glucoside
  • 2,3,5,4'-TETRAHYDROXYSTILBENE-2-O-B-D-GLUCOPYRANOSIDE
  • b-D-Glucopyranoside,2,4-dihydroxy-6-[(1E)-2-(4-hydroxyphenyl)ethenyl]phenyl
  • CIS,2,3,5,4-tetrahydroxyl diphenylethylene-2-o-glucoside
  • 2,3,4,5,6-PENTAFLUOROPHENYL4-BROMO-2-CHLOROBENZENESULFONATE
  • 2,3,5,4'-tetera-hydroxystilbenen-2-O-Beta-D-glucoside
  • 2,3,5,4'-tetrahydroxystibene-2-O-Beta-D glucoside
  • 2,3,5,4'-Tetrahydroxystilbene-2-O-β-D-glucopyranoside
  • 2,4-Dihydroxy-6-[(1E)-2-(4-hydroxyphenyl)ethenyl]phenyl β-D-Glucopyranoside
  • EH-201
  • THSG
  • Tetrahydroxystilbene glucoside
  • 2,3,5,4′-Tetrahydroxystilbene 2-O-β-D-glucoside
  • 2,3,5,4'-Tetrahydroxy;stilbene-2-Ο-β-D- glucoside
  • Tetrahydroxystilbene Glucoside
  • 2,3,5,4'-Tetra-hydroxystilbene-2-O-beta-D-glucopyranoside
  • Astragalus polyphenols
  • 2,3,5,4-tetrahydroxyl diphenylethylene-2-o-glucoside
  • 54QRI6OKJ5
  • 2,3,5,4'-Tetrahydroxystilbene-2-O-beta-D-glucoside
  • (2S,3R,4S,5S,6R)-2-(2,4-dihydroxy-6-((E)-4-hydroxystyryl)phenoxy)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol
  • (2S,3R,4S,5S,6R)-2-[2,4-dihydroxy-6-[(E)-2-(4-hydroxyphenyl)ethenyl]phenoxy]-6-(hydroxymeth
  • (2S,3R,4S,5S,6R)-2-[2,4-dihydroxy-6-[(E)-2-(4-hydroxyphenyl)ethenyl]phenoxy]-6-(hydroxymethyl)oxane-
  • 2,4-Dihydroxy-6-[(1E)-2-(4-hydroxyphenyl)ethenyl]phenyl β-D-glucopyranoside (ACI)
  • β-D-Glucopyranoside, 2,4-dihydroxy-6-[2-(4-hydroxyphenyl)ethenyl]phenyl, (E)- (ZCI)
  • (E)-2,3,5,4′-Tetrahydroxy stilbene-2-O-glucoside
  • 2,3,4′,5-Tetrahydroxystilbene 2-O-D-glucoside
  • trans-2,3,5,4′-Tetrahydroxystilbene-2-O-β-d-glucopyranoside
  • 2,3,5,4'-Tetrahydroxystilbene 2-O--D-glucoside
  • MFCD00238694
  • CCG-268716
  • AfAE'Adaggeratrade markAfA centA centasA notA em leaderA inverted exclamation mark-D-glucoside
  • SCHEMBL2688101
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-glucosid
  • 2,3,5,4'-Tetrahydroxytoluylene-2-beta-D-glucopyranoside
  • 2,4-dihydroxy-6-[(E)-2-(4-hydroxyphenyl)ethenyl]phenyl beta-D-glucopyranoside
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-fA-D-Glucoside
  • Q-100633
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-b-D-glucoside
  • 2,3,5,4'-Tetrahydroxytoluylene-2-beta-D-glucoside
  • CHEBI:140850
  • tetrahydroxyldiphenylethylene-2-o-glucoside
  • s3906
  • (E)-2,3,5,4'-tetrahydroxystilbene-2-O-beta-D-glucoside
  • 2,3,5,4'-Tetrahydroxyl diphenylethylene-2-O-glucoside
  • 2,3,5,4'-TETRAHYDROXYSTILBENE-2-O-.BETA.-D-GLUCOSIDE
  • AC-33974
  • F16062
  • 2,3,5,4'-Tetrahydroxy stilbene-2---D-glucoside
  • 2,3,5,4'-tetrahydroxystilbene 2-O-beta-D-glucoside
  • trans-2,3,5,4'-tetrahydroxystilbene-2-O-beta-D-glucoside
  • DTXSID801242061
  • AKOS030530177
  • (2S,3R,4S,5S,6R)-2-[2,4-dihydroxy-6-[(E)-2-(4-hydroxyphenyl)ethenyl]phenoxy]-6-(hydroxymethyl)oxane-3,4,5-triol
  • 2,3,5,4-tetrahydroxyl-diphenylethylene-2-o-glucoside
  • UNII-54QRI6OKJ5
  • 2,3,5,4'-tetrahydroxystilbene-2-o-beta-d-glucopyranoside
  • 55327-45-2
  • NCGC00482790-01
  • A864422
  • BDBM50020713
  • 2,3,5,4'-TETRAHYDROXYSTILBENE-2-O-BETA-D-GLUCOSIDE (USP-RS)
  • T3513
  • W-203871
  • 2,3,5,4'-TETRAHYDROXYSTILBENE-2-O-BETA-D-GLUCOSIDE [USP-RS]
  • SCHEMBL17507729
  • 2,4-DIHYDROXY-6-((1E)-2-(4-HYDROXYPHENYL)ETHENYL)PHENYL .BETA.-D-GLUCOPYRANOSIDE
  • 2,3,5,4'-Tetrahydroxystilbene 2-O-AfAE'A centa' notA inverted exclamation markAfasA'A
  • 2,3,5,4-Tetrahydroxy stilbene-2-Omicron-beta-D-glucoside
  • beta-D-Glucopyranoside, 2,4-dihydroxy-6-((1E)-2-(4-hydroxyphenyl)ethenyl)phenyl
  • 2,3,5,4'-Tetrahydroxyl-diphenylethylene-2-O-beta-D-glucoside
  • tetrahydroxyl diphenylethylene-2-o-gluco
  • 2,3,4',5-Tetrahydroxystilbene 2-o-D-glucoside
  • CHEMBL460860
  • 2,3,5,4'-Tetrahydroxystilbene-2-O-ss-D-glucoside
  • AKOS040758637
  • 82373-94-2
  • B-D-GLUCOPYRANOSIDE,2,4-DIHYDROXY-6-[2-(4-HYDROXYPHENYL)ETHENYL]PHENYL
  • tetrahydroxystilbene glucoside
  • 2,3,5,4'-Tetrahydroxystilbene-2-O-b-D-glucopyranoside
  • 2,4-Dihydroxy-6-((1E)-2-(4-hydroxyphenyl)ethenyl)phenyl beta-D-glucopyranoside
  • beta-D-Glucopyranoside, 2,4-dihydroxy-6-(2-(4-hydroxyphenyl)ethenyl)phenyl
  • Tetrahydroxystilbene-2-O-??-D-glucoside
  • (2S,3R,4S,5S,6R)-2-[2,4-dihydroxy-6-[(E)-2-(4-hydroxyphenyl)vinyl]phenoxy]-6-(hydroxymethyl)tetrahydropyran-3,4,5-triol
  • 2,3,4',5-Tetrahydroxystilbene 2-O-Glucoside
  • .BETA.-D-GLUCOPYRANOSIDE, 2,4-DIHYDROXY-6-((1E)-2-(4-HYDROXYPHENYL)ETHENYL)PHENYL
  • .BETA.-D-GLUCOPYRANOSIDE, 2,4-DIHYDROXY-6-(2-(4-HYDROXYPHENYL)ETHENYL)PHENYL, (E)-
  • beta-D-Glucopyranoside, 2,4-dihydroxy-6-(2-(4-hydroxyphenyl)ethenyl)phenyl, (E)-
  • (E)-2,3,5,4'-Tetrahydroxy stilbene-2-O-glucoside
  • 2,3,5,4'-tetrahydroxystilbene-2-O-?-D-glucoside
  • AS-76404
  • [ "" ]
  • 2,3,4',5-Tetrahydroxystilbene 2-O-beta-D-glucopyranoside
  • 2,3,5,4'-tetrahydroxystilbene-2-O-beta-D-glucoside
  • MDL:MFCD00238694
  • InChIKey:JAYVHSBYKLLDJC-DSNJPTTOSA-N
  • Inchi:1S/C20H22O9/c21-9-15-16(25)17(26)18(27)20(28-15)29-19-11(7-13(23)8-14(19)24)4-1-10-2-5-12(22)6-3-10/h1-8,15-18,20-27H,9H2/b4-1+/t15-,16-,17+,18-,20+/m1/s1
  • SMILES:O([C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1)C1=C(O)C=C(O)C=C1/C=C/C1C=CC(O)=CC=1
Chemical and Physical Properties

Computed Properties

  • Exact Mass: 406.4g/mol
  • Surface Charge: 0
  • XLogP3: 1
  • Hydrogen Bond Donor Count: 7
  • Hydrogen Bond Acceptor Count: 9
  • Rotatable Bond Count: 5
  • Monoisotopic Mass: 406.126382g/mol
  • Monoisotopic Mass: 406.126382g/mol
  • Topological Polar Surface Area: 160Ų
  • Heavy Atom Count: 29
  • Complexity: 536
  • Isotope Atom Count: 0
  • Defined Atom Stereocenter Count: 5
  • Undefined Atom Stereocenter Count : 0
  • Defined Bond Stereocenter Count: 1
  • Undefined Bond Stereocenter Count: 0
  • Covalently-Bonded Unit Count: 1

Experimental Properties

  • LogP: 0.15250
  • PSA: 160.07000
  • Solubility: H2O: soluble5mg/mL, clear (warmed)
  • Color/Form: Powder
  • Boiling Point: 715°C at 760 mmHg
  • Refractive Index: 1.76
  • Flash Point: 386.2°C
  • Density: 1.593g/cm3
Security Information
  • Symbol: GHS07
  • WGK Germany:3
  • Safety Instruction:26
  • Dangerous goods sign: Xi Xi
  • Hazardous Material transportation number:NONH for all modes of transport
  • Hazard Statement:H315-H319
  • Warning Statement:P305+P351+P338
  • Storage Condition:Powder -20°C 3 years   4°C 2 years In solvent -80°C 6 months   -20°C 1 month
  • Hazard Category Code:36/38
  • Signal Word:Warning
Synthetic Circuit

Synthetic Circuit 1

Reaction Conditions
1.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
1.2 rt; 12 h, rt
1.3 Solvents: Water ;  rt
2.1 Reagents: Sodium borohydride Solvents: Methanol ;  30 min, rt
2.2 Reagents: Hydrochloric acid Solvents: Water ;  rt
3.1 Reagents: Carbon tetrabromide ,  Triphenylphosphine Solvents: Diethyl ether ;  rt
4.1 Solvents: Toluene ;  12 h, reflux
5.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
5.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
5.3 Solvents: Water ;  rt
6.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
6.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
7.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
7.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 2

Reaction Conditions
1.1 Reagents: Carbon tetrabromide ,  Triphenylphosphine Solvents: Diethyl ether ;  rt
2.1 Solvents: Toluene ;  12 h, reflux
3.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
3.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
3.3 Solvents: Water ;  rt
4.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
4.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
5.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
5.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 3

Reaction Conditions
1.1 Reagents: Sodium borohydride Solvents: Methanol ;  30 min, rt
1.2 Reagents: Hydrochloric acid Solvents: Water ;  rt
2.1 Reagents: Carbon tetrabromide ,  Triphenylphosphine Solvents: Diethyl ether ;  rt
3.1 Solvents: Toluene ;  12 h, reflux
4.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
4.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
4.3 Solvents: Water ;  rt
5.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
5.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
6.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
6.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 4

Reaction Conditions
1.1 Reagents: Potassium carbonate Solvents: Acetone ;  reflux
2.1 Reagents: Hydrogen peroxide Catalysts: Sulfuric acid Solvents: Methanol ,  Water ;  2 h, rt
2.2 Solvents: Water ;  rt
3.1 Solvents: Acetic acid ,  Dimethylformamide ;  3 h, reflux
3.2 Solvents: Water
4.1 Reagents: Sodium hydroxide Catalysts: Tetrabutylammonium bromide Solvents: Dichloromethane ,  Water ;  12 h, 65 - 70 °C
4.2 Solvents: Water
5.1 Reagents: Hydrogen Catalysts: Palladium Solvents: Ethyl acetate ;  16 h, 45 psi, rt
6.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
7.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
7.2 rt; 15 h, rt
7.3 Solvents: Water ;  rt
8.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
8.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
8.3 Solvents: Water ;  rt
9.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
9.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
10.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
10.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 5

Reaction Conditions
1.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
1.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
2.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
2.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 6

Reaction Conditions
1.1 Reagents: Hydrogen Catalysts: Palladium Solvents: Ethyl acetate ;  16 h, 45 psi, rt
2.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
3.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
3.2 rt; 15 h, rt
3.3 Solvents: Water ;  rt
4.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
4.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
4.3 Solvents: Water ;  rt
5.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
5.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
6.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
6.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 7

Reaction Conditions
1.1 Solvents: Acetic acid ,  Dimethylformamide ;  3 h, reflux
1.2 Solvents: Water
2.1 Reagents: Sodium hydroxide Catalysts: Tetrabutylammonium bromide Solvents: Dichloromethane ,  Water ;  12 h, 65 - 70 °C
2.2 Solvents: Water
3.1 Reagents: Hydrogen Catalysts: Palladium Solvents: Ethyl acetate ;  16 h, 45 psi, rt
4.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
5.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
5.2 rt; 15 h, rt
5.3 Solvents: Water ;  rt
6.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
6.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
6.3 Solvents: Water ;  rt
7.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
7.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
8.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
8.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 8

Reaction Conditions
1.1 Solvents: Toluene ;  12 h, reflux
2.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
2.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
2.3 Solvents: Water ;  rt
3.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
3.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
4.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
4.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 9

Reaction Conditions
1.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
2.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
2.2 rt; 15 h, rt
2.3 Solvents: Water ;  rt
3.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
3.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
3.3 Solvents: Water ;  rt
4.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
4.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
5.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
5.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 10

Reaction Conditions
1.1 Reagents: Sodium hydroxide Catalysts: Tetrabutylammonium bromide Solvents: Dichloromethane ,  Water ;  12 h, 65 - 70 °C
1.2 Solvents: Water
2.1 Reagents: Hydrogen Catalysts: Palladium Solvents: Ethyl acetate ;  16 h, 45 psi, rt
3.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
4.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
4.2 rt; 15 h, rt
4.3 Solvents: Water ;  rt
5.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
5.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
5.3 Solvents: Water ;  rt
6.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
6.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
7.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
7.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 11

Reaction Conditions
1.1 Catalysts: Water Solvents: Methanol ;  0.5 h
Reference
Water-Assisted/Water-Accelerated Photoreaction of trans-2,3,4',5-Tetrahydroxystilbene-2-O-β-D-glucoside from the Roots of Polygonum multiflorum
Bao, Ni-Man ; et al, Journal of Agricultural and Food Chemistry, 2020, 68(18), 5086-5092

Synthetic Circuit 12

Reaction Conditions
1.1 Reagents: Hydrogen peroxide Catalysts: Sulfuric acid Solvents: Methanol ,  Water ;  2 h, rt
1.2 Solvents: Water ;  rt
2.1 Solvents: Acetic acid ,  Dimethylformamide ;  3 h, reflux
2.2 Solvents: Water
3.1 Reagents: Sodium hydroxide Catalysts: Tetrabutylammonium bromide Solvents: Dichloromethane ,  Water ;  12 h, 65 - 70 °C
3.2 Solvents: Water
4.1 Reagents: Hydrogen Catalysts: Palladium Solvents: Ethyl acetate ;  16 h, 45 psi, rt
5.1 Reagents: Dipyridinium dichromate Solvents: Dichloromethane ;  12 h, rt
6.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
6.2 rt; 15 h, rt
6.3 Solvents: Water ;  rt
7.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
7.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
7.3 Solvents: Water ;  rt
8.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
8.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
9.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
9.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 13

Reaction Conditions
1.1 Reagents: Diisopropylethylamine Solvents: Dichloromethane ;  10 min, rt
1.2 rt; 15 h, rt
1.3 Solvents: Water ;  rt
2.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
2.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
2.3 Solvents: Water ;  rt
3.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
3.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
4.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
4.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 14

Reaction Conditions
1.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -78 °C; 30 min, -78 °C; -78 °C → rt; 1 h, rt; rt → -78 °C
1.2 Solvents: Tetrahydrofuran ;  1 h, -78 °C; 18 h, rt
1.3 Solvents: Water ;  rt
2.1 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  1.5 h, 0 °C
2.2 Reagents: Hydrochloric acid Solvents: Water ;  0 °C
3.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
3.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301

Synthetic Circuit 15

Reaction Conditions
1.1 Reagents: Potassium hydroxide Solvents: Ethanol ;  40 min, rt
1.2 Solvents: Water ;  rt
Reference
Total Synthesis of Two Glycosylated Stilbenes, Oxyresveratrol 2-O-β-D-Glucopyranoside and 2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-Glucopyranoside
Kumar, Sunil; et al, Journal of Natural Products, 2017, 80(5), 1294-1301
Related Literature
  • 1. Enhanced TSG stability through co-assembly with C3G: the mechanism behind processing Polygonum multiflorum Thunb with black beans via supramolecular analysis Yue Liu,Shukai Wang,Yunan Qin,Ying Wang,Jianbo Yang,Lanzhen Zhang,Quan Li,Shuangcheng Ma Food Funct. 2023 14 4204
Related Products
Price Data Available
Brand:Mce Supplier:MedChemExpress
No. Purity Stock Specification Price update time operate
HY-N0652-10mM*1mLinDMSO 99.20% In-stock 10mM*1mLinDMSO ¥550 26 Jul. 2023
HY-N0652-10mg 99.20% In-stock 10mg ¥500 01 Sep. 2023
HY-N0652-25mg 99.20% In-stock 25mg ¥1000 01 Sep. 2023
HY-N0652-50mg 99.20% In-stock 50mg ¥1400 01 Sep. 2023
HY-N0652-5mg 99.20% In-stock 5mg ¥312 01 Sep. 2023
HY-N0652-10mM*1 mL in DMSO 99.20% In-stock 10mM*1 mL in DMSO ¥550 01 Sep. 2023
Brand:sigmaaldrich Supplier:西格玛奥德里奇(上海)贸易有限公司
No. Purity Stock Specification Price update time operate
PHL82666-10MG 10mg ¥4932.81 09 Sep. 2023
1651654-50MG 50MG ¥4896.69 12 Apr. 2023
PHL82666-10MG 10MG ¥4697.92 06 Jan. 2023
1651654-50MG 50mg ¥5141.51 06 Sep. 2023
Brand:dcchemical Supplier:DC Chemicals
No. Purity Stock Specification Price update time operate
DCS-029-20 mg >98%, Standard References Grade In stock 20mg $280.0/ ¥2,033.70 01 Mar. 2022
DCS-029-20mg >98%, Standard References Grade In stock 20mg $280.0/ ¥2,033.70 15 Sep. 2023
Brand:abcr Supplier:abcr
No. Purity Stock Specification Price update time operate
AB294879-250mg 250mg €141.50/ ¥1,026.04 08 Sep. 2023
AB294879-1g 1g €242.80/ ¥1,760.59 08 Sep. 2023
AB294879-1 g 1 g €242.80/ ¥1,760.59 20 Jul. 2023
AB294879-250 mg 250 mg €141.50/ ¥1,026.04 20 Jul. 2023
Brand:a2bchem Supplier:A2B Chem LLC
No. Purity Stock Specification Price update time operate
AC37593-250mg ≥98% in stock 250mg $510.00/ ¥3,704.23 30 Dec. 2023
AC37593-50mg 99% in stock 50mg $112.00/ ¥813.48 30 Dec. 2023
AC37593-25mg 99% in stock 25mg $80.00/ ¥581.06 30 Dec. 2023
AC37593-10mg 99% in stock 10mg $40.00/ ¥290.53 30 Dec. 2023
AC37593-5mg 99% in stock 5mg $26.00/ ¥188.84 30 Dec. 2023
Brand:1pchem Supplier:1PlusChem
No. Purity Stock Specification Price update time operate
1P0053Y1-250mg ≥98% 1 week 250mg $651.00/ ¥4,728.34 16 Dec. 2023
1P0053Y1-100mg ≥98% 1 week 100mg $335.00/ ¥2,433.17 16 Dec. 2023
1P0053Y1-50mg 99% 1 week 50mg $191.00/ ¥1,387.27 16 Dec. 2023
1P0053Y1-25mg ≥98% 1 week 25mg $138.00/ ¥1,002.32 16 Dec. 2023
1P0053Y1-10mg 99% 1 week 10mg $91.00/ ¥660.95 16 Dec. 2023
1P0053Y1-5mg 99% 1 week 5mg $81.00/ ¥588.32 16 Dec. 2023
Brand:aaron Supplier:Aaron
No. Purity Stock Specification Price update time operate
AR00546D-5g 98% In China Stock 5g $517.00/ ¥3,755.07 13 Dec. 2023
AR00546D-1g 98% In China Stock 1g $130.00/ ¥944.22 13 Dec. 2023
AR00546D-250mg 98% In China Stock 250mg $57.00/ ¥414.00 13 Dec. 2023
AR00546D-100mg 98% In China Stock 100mg $31.00/ ¥225.16 13 Dec. 2023
Brand:phytolab Supplier:PhytoLab
No. Purity Stock Specification Price update time operate
82666-1000mg ≥ 95.0 % 1000mg €13800/ ¥100,066.56 25 Oct. 2023
82666-500mg ≥ 95.0 % 500mg €7360/ ¥53,368.83 25 Oct. 2023
82666-250mg ≥ 95.0 % 250mg €3910/ ¥28,352.19 25 Oct. 2023
82666-50mg ≥ 95.0 % 50mg €827.9999999999999/ ¥6,003.99 25 Oct. 2023
Brand:nstchemcial Supplier:Nature Science Technologies
No. Purity Stock Specification Price update time operate
NST-10-1-25g 98% (HPLC) 25g € 520/ ¥3,770.62 21 Sep. 2023
NST-10-1-10g 98% (HPLC) 10g € 230/ ¥1,667.78 21 Sep. 2023
NST-10-1-5g 98% (HPLC) 5g € 160/ ¥1,160.19 21 Sep. 2023
NST-10-1-2.52,5g 98% (HPLC) 2.52,5g € 110/ ¥797.63 21 Sep. 2023
NST-10-1-25 g 98% (HPLC) 25g € 520/ ¥3,770.62 10 Jul. 2023
NST-10-1-10 g 98% (HPLC) 10g € 230/ ¥1,667.78 10 Jul. 2023
NST-10-1-5 g 98% (HPLC) 5g € 160/ ¥1,160.19 10 Jul. 2023
NST-10-1-2,5 g 98% (HPLC) 2,5 g € 110/ ¥797.63 10 Jul. 2023
Brand:scbt Supplier:圣克鲁斯生物技术
No. Purity Stock Specification Price update time operate
sc-283376A-2g 2g ¥12974.00 05 Sep. 2023
sc-283376-500mg 500mg ¥6017.00 05 Sep. 2023
sc-283376A-2 g 2g ¥12,974.00 10 Jul. 2023
sc-283376-500 mg 500MG ¥6,017.00 10 Jul. 2023
Brand:targetmol Supplier:TargetMol Chemicals
No. Purity Stock Specification Price update time operate
T2964-1 mL * 10 mM (in DMSO) 99.77% 上海现货 1 mL * 10 mM (in DMSO) ¥ 410 11 Jul. 2023
T2964-100 mg 99.77% 上海现货 100MG ¥ 1,730 11 Jul. 2023
T2964-50 mg 99.77% 上海现货 50mg ¥ 1,156 11 Jul. 2023
T2964-25 mg 99.77% 上海现货 25mg ¥ 811 11 Jul. 2023
T2964-10 mg 99.77% 上海现货 10mg ¥ 410 11 Jul. 2023
Brand:enovation Supplier:eNovation Chemicals LLC
No. Purity Stock Specification Price update time operate
Y1291321-1g 98% 1g $215/ ¥1,561.59 17 May. 2023
D659438-20mg 98% 20mg $285/ ¥2,070.01 03 Sep. 2023
Brand:TCI Supplier:梯希爱(上海)化成工业发展有限公司
No. Purity Stock Specification Price update time operate
T3513-250MG >98.0%(HPLC) 上海:请联系我们/天津:请联系我们/日本:20 250mg ¥1100.00 07 Sep. 2023
T3513-50MG >98.0%(HPLC) 上海:请联系我们/天津:请联系我们/日本:10 50mg ¥350.00 07 Sep. 2023
Brand:麦克林 Supplier:上海麦克林生化科技有限公司
No. Purity Stock Specification Price update time operate
T874838-1g 99% 预计交期:8~10个工作日 1g ¥1,692.00 28 Sep. 2022
T874838-500mg 99% 预计交期:1个工作日 500mg ¥1,128.00 28 Sep. 2022
T874838-100mg 99% 上海仓库:现货/北方仓库:现货/南方仓库:- 100mg ¥310.00 28 Sep. 2022
Brand:韶远 Supplier:上海韶远试剂有限公司
No. Purity Stock Specification Price update time operate
SY022367-10mg 98% 10mg ¥405.0 15 Sep. 2023
Brand:罗恩试剂 Supplier:上海易恩化学技术有限公司
No. Purity Stock Specification Price update time operate
R097435-500mg 99% 现货 500mg ¥654 07 Sep. 2023
R097435-100mg 99% 现货 100mg ¥204 07 Sep. 2023
R027737-20mg 98%(分析标准试剂) 现货 20mg ¥338 07 Sep. 2023
Brand:百灵威 Supplier:百灵威科技有限公司
No. Purity Stock Specification Price update time operate
910360-22MG 22MG ¥ 377 26 Apr. 2022
928007-5MG 98% 河北: 4 5MG ¥ 125 26 Apr. 2022
Brand:chemfaces Supplier:ChemFaces
No. Purity Stock Specification Price update time operate
CFN99995-20mg >=98% 20mg $30/ ¥217.90 19 Sep. 2023
CFN99995-20mg >=98% 20mg $40/ ¥290.53 22 Jul. 2021
Brand:topscience Supplier:上海陶术生物科技有限公司
No. Purity Stock Specification Price update time operate
T2964-1 mL * 10 mM (in DMSO) 99.77% 上海现货 1 mL * 10 mM (in DMSO) ¥410.00 26 Apr. 2022
T2964-100 mg 99.77% 上海现货 100MG ¥1730.00 26 Apr. 2022
T2964-50 mg 99.77% 上海现货 50mg ¥1156.00 26 Apr. 2022
T2964-25 mg 99.77% 上海现货 25mg ¥811.00 26 Apr. 2022
T2964-10 mg 99.77% 上海现货 10mg ¥410.00 26 Apr. 2022
Brand:Biopurify Supplier:Chengdu Biopurify Phytochemicals Ltd
No. Purity Stock Specification Price update time operate
BP0039-20mg 98% 20mg $40/ ¥290.53 20 Sep. 2023
BP0039-100mg 98% 100mg $80/ ¥581.06 20 Sep. 2023
BP0039-1000mg 98% 1000mg $160/ ¥1,162.11 20 Sep. 2023
Brand:安捷凯 Supplier:武汉安捷凯生物医药科技有限公司
No. Purity Stock Specification Price update time operate
ajcn5494-20mg 98% 现货 20mg ¥1269.00 07 Sep. 2023
Brand:Acmec Supplier:上海吉至生化科技有限公司
No. Purity Stock Specification Price update time operate
T88670-1g 现货 1g ¥3498.0 07 Sep. 2021
T88670-20mg 现货 20mg ¥278.0 07 Sep. 2021
Brand:源叶 Supplier:上海源叶生物科技有限公司
No. Purity Stock Specification Price update time operate
B21757-1g 分析标准品,HPLC≥98% 上海:准现货/北京:0/武汉:0/南京:0 1g ¥3500.00 02 Sep. 2021
B21757-20mg 分析标准品,HPLC≥98% 上海:>10/北京:2/武汉:4/南京:3 20mg ¥280.00 02 Sep. 2021
Brand:bomeibio Supplier:合肥博美生物科技有限责任公司
No. Purity Stock Specification Price update time operate
BZP0269-20mg HPLC≥98% 现货 20mg ¥320元 15 Sep. 2023
Brand:aladdin Supplier:上海阿拉丁生化科技股份有限公司
No. Purity Stock Specification Price update time operate
T110192-20mg 分析标准品,>98% 现货 20mg ¥352.90 01 Sep. 2023
Brand:九鼎 Supplier:上海贤鼎生物科技有限公司
No. Purity Stock Specification Price update time operate
CG191-5mg 95+% 3~5天 5mg 542CNY 08 May. 2021
CG191-10mg 95+% 3~5天 10mg 898CNY 08 May. 2021
CG191-25mg 95+% 3~5天 25mg 1797CNY 08 May. 2021
The above data is all sourced from the internet. If privacy is violated, please contact us as soon as possible (leave a copy of your company email), and we will take it down for processing! Sorry for any inconvenience caused!
©2008-2024 chem960.com All rights reserved