找化学品上960化工网!
960化工网

9-氨基菲 | 947-73-9

9-氨基菲
9-Aminophenanthrene
947-73-9
C14H11N
193.243843317032
如需查看该化合物的详细结构式,mol文件,smile,InChi 请点击:9-氨基菲结构式
9-氨基菲MSDS
24848932
9-氨基菲价格
名称和标识符
MDL MFCD00001177
InChIKey KIHQWOBUUIPWAN-UHFFFAOYSA-N
Inchi 1S/C14H11N/c15-14-9-10-5-1-2-6-11(10)12-7-3-4-8-13(12)14/h1-9H,15H2
SMILES NC1C2C(=CC=CC=2)C2C(=CC=CC=2)C=1
别名信息
- 中文别名 -
  • 9-氨基菲
  • 2-菲胺
  • 9-氨菲
  • 9-菲胺
- 英文别名 -
  • 9-Aminophenanthrene
  • 9-AMINO PHENANTHRANE
  • 2-aminophenanthrene
  • 9-aminophenantrene
  • 9-PHENANTHRENAMINE
  • 9-Phenanthrylamine
  • Phenanthren-9-ylaMine
  • Phenanthrylamine
  • 9-Phenanthrylamine (6CI, 7CI, 8CI)
  • (Phenanthren-9-yl)amine
  • Phenanthren-9-amine
物化性质
实验特性
LogP 4.15640
PSA 26.02000
折射率 1.5850 (estimate)
水溶性 It is slightly soluble in water 0.00581 mg/mL.
沸点 319.47°C (rough estimate)
熔点 137-139 °C (lit.)
蒸气压 0.0±1.0 mmHg at 25°C
闪点 224.4±15.4 °C
颜色与性状 未确定
溶解性 未确定
密度 1.1061 (rough estimate)
计算特性
精确分子量 193.08900
氢键供体数量 1
氢键受体数量 1
可旋转化学键数量 0
重原子数量 15
复杂度 225
同位素原子数量 0
确定原子立构中心数量 0
不确定原子立构中心数量 0
确定化学键立构中心数量 0
不确定化学键立构中心数量 0
共价键单元数量 1
疏水参数计算参考值(XlogP)
互变异构体数量
表面电荷 0
国际标准相关数据
EINECS 213-431-6
海关数据
海关编码 2921499090
海关数据

中国海关编码:

2921499090

概述:

2921499090 其他芳香单胺及衍生物及它们的盐. 增值税率:17.0% 退税率:9.0% 监管条件:无 最惠国关税:6.5% 普通关税:30.0%

申报要素:

品名, 成分含量, 用途

Summary:

2921499090 other aromatic monoamines and their derivatives; salts thereof VAT:17.0% Tax rebate rate:9.0% Supervision conditions:none MFN tariff:6.5% General tariff:30.0%

合成路线

合成路线:1 步

反应条件:
参考文献:
Efficient Synthesis of 9-Aminophenanthrenes and Heterocyclic Analogues by Electrocyclization of Biaryl Keteniminium Salts
Quinodoz, Pierre ; Kolleth, Amandine; Dagoneau, Dylan ; Yoshimura, Masahiko; Reyes Mendez, Lucia; et al, Helvetica Chimica Acta, 2022, 105(11),

合成路线:1 步

反应条件:
参考文献:
A different route to the synthesis of 9,10-disubstituted phenanthrenes
Tempesti, Tomas C.; Pierini, Adriana B.; Baumgartner, Maria T., Journal of Organic Chemistry, 2005, 70(16), 6508-6511

合成路线:1 步

反应条件:
参考文献:
Transition-Metal-Free Access to Primary Anilines from Boronic Acids and a Common +NH2 Equivalent.
Voth, Samantha; Hollett, Joshua W.; McCubbin, J. Adam, Journal of Organic Chemistry, 2015, 80(5), 2545-2553

合成路线:1 步

反应条件:
参考文献:
Novel substituted heterocyclic compounds as electroluminescent host material for an organic electroluminescent device
, Korea, , ,

合成路线:1 步

反应条件:
参考文献:
Deacetylative Amination of Acetyl Arenes and Alkanes with C-C Bond Cleavage
Hyodo, Kengo ; Hasegawa, Genna; Maki, Hiroya; Uchida, Kingo, Organic Letters, 2019, 21(8), 2818-2822

合成路线:1 步

反应条件:
参考文献:
Electrochemical oxidation induced intermolecular aromatic C-H imidation
Hu, Xia; Zhang, Guoting; Nie, Lei; Kong, Taige; Lei, Aiwen, Nature Communications, 2019, 10(1), 1-10

合成路线:1 步

反应条件:
参考文献:
A new cyclization reaction
Bradsher, Charles K.; Beavers, Dorothy J.; Little, Edwin D., Journal of the American Chemical Society, 1954, 76,

合成路线:1 步

反应条件:
参考文献:
Mild and Highly Selective Palladium-Catalyzed Monoarylation of Ammonia Enabled by the Use of Bulky Biarylphosphine Ligands and Palladacycle Precatalysts
Cheung, Chi Wai; Surry, David S.; Buchwald, Stephen L., Organic Letters, 2013, 15(14), 3734-3737

合成路线:1 步

反应条件:
参考文献:
Elusive Metal-Free Primary Amination of Arylboronic Acids: Synthetic Studies and Mechanism by Density Functional Theory
Zhu, Chen; Li, Gongqiang; Ess, Daniel H.; Falck, John R.; Kurti, Laszlo, Journal of the American Chemical Society, 2012, 134(44), 18253-18256

合成路线:1 步

反应条件:
参考文献:
New route to 9-phenanthrylamine
Altiparmakian, R. H.; Braithwaite, Richard S. W., Journal of the Chemical Society [Section] C: Organic, 1967, (19),

合成路线:1 步

反应条件:
参考文献:
New synthetic route to 9,10-iminophenanthrene
Denis, J. N.; Krief, A., Tetrahedron, 1979, 35(24), 2901-3

合成路线:1 步

反应条件:
参考文献:
Monoamine derivatives for use as hole transfer layers in organic electroluminescent devices
, United States, , ,

合成路线:1 步

反应条件:
参考文献:
Material for organic electroluminescent device and organic electroluminescent device including the same
, United States, , ,

合成路线:1 步

反应条件:
参考文献:
Monoamine derivatives having dibenzothiophene structures and organic electroluminescence devices using them
, Japan, , ,

合成路线:1 步

反应条件:
参考文献:
Derivatives of phenanthrene. The preparation of 9-amino-, 9-iodo-, and 9-fluorophenanthrene
Goldberg, M. A.; Ordas, E. P.; Carsch, G., Journal of the American Chemical Society, 1947, 69, 260-2

合成路线:1 步

反应条件:
参考文献:
Aryl amine derivative and application in organic electroluminescent device
, China, , ,

合成路线:1 步

反应条件:
参考文献:
Synthesis of triaryls: hydroxy and amine dinaphthyl and diphenanthryl aryls by one-pot electron-transfer nucleophilic substitution reactions
Jimenez, Liliana B.; Torres, Natalia V.; Borioni, Jose L.; Pierini, Adriana B., Tetrahedron, 2014, 70(22), 3614-3620

合成路线:1 步

反应条件:
参考文献:
Nickel-Catalyzed Synthesis of Primary Aryl and Heteroaryl Amines via C-O Bond Cleavage
Yue, Huifeng; Guo, Lin; Liu, Xiangqian; Rueping, Magnus, Organic Letters, 2017, 19(7), 1788-1791

合成路线:1 步

反应条件:
参考文献:
Mono amine derivatives and organic electroluminescent device including the same
, United States, , ,

合成路线:1 步

反应条件:
参考文献:
Materials for organic electroluminescent devices for improved emission life, and organic electroluminescent devices using the materials
, United States, , ,
相关文献
专业数据库参考
PubChemId 24848932
参考资料
Reaxys RN
960化工网为您提供9-氨基菲专业化合物百科信息,包括中文名,英文名,分子式,分子量,以及该化合物的CasNo.:947-73-9,和相关理化性质;并提供了优质生产厂家信息包括厂家名称和联系方式等;| WAP 版:947-73-9
平台客服 平台客服

平台在线客服