1.1
Reagents:
Tetrabutylammonium iodide
,
Diethyl phosphate
Catalysts:
Triphenylphosphine
,
Di-μ-chlorobis[(1,2,5,6-η)-1,3,5,7-cyclooctatetraene]dirhodium
Solvents:
N-Methyl-2-pyrrolidone
,
1,1,1,3,3,3-Hexafluoro-2-propanol
;
rt; 24 h, 5 bar, 110 °C; 110 °C → rt
1.2
Reagents:
Water
;
rt